Chemistry 103/113 Laboratory

 

 

This Week

Answer Keys

Gen Chem Lab

Periodic Table

 

 

 

·       Expt 6:  Photochemical Blues (week 2)

o      Week 2 report due tomorrow

 

Next Time

·       Expt 6:  Photochemical Blues (week 3)

·       Quiz 4:  Expts 4, 8

 

Notes for Today

Photochemical Blues (Week 2)

·       Overview: 

o      Synthesize/purify K3Fe(C2O4)3.3H2O (“Green Compound”) (Week 1)

o      Qualitative tests for K+, Fe3+, C2O42- (Week 2)

o      %Fe photoreduction assay (Weeks 2,3)

o      Make blueprints (Week 3)

 

·       Qualitative Tests of the Green Compound:

o      Precipitation tests for Fe3+ and C2O42-

o      Flame test for K+

§       heat excites electrons to high E levels

§       as electrons drop back to lower E levels, photons of light are emitted

                           

 

§       light color emitted is determined by element’s electron E level spacings

color emitted depends on the element

                

 

·       Quantitative Analysis of the Green Compound for Mass %Fe3+:

                

o      Today

§       Weigh green solid, dissolve, expose to light

o      Next Time

§       Collect and weigh the FeC2O4.2H2O produced from green solid

§       Find moles FeC2O4.2H2O produced

§       Find moles Fe3+ present in the green solid

§       Find grams Fe3+in the green solid

 

·       Safety Issues

o      Splash hazard.  Goggles required.

o      Bunsen burner