Chemistry 211, Schedule for Semester I, Fall 2011

	Dates	Experiment #	Experiment Title	Experiment Type
General Lab Information (docx) (pdf) Forces and Factors (docx) (pdf) Laboratory Equipment
	May 29, 30	Experiment 1a (docx) Experiment 1a (pdf)	General Lab Information Gas Chromatography/Steam Distillation Check-in YouTube Orientation/Safety Lecture-thermal burn and cut safety General safety: Chemical exposure: Fire safety: Thermal Cuts and Burns: How to Build a Proper Still: part I How to Build a Proper Still: part II How to Run a Basic GC Images Apparatus 1 Apparatus 2	I ^{1, 2}
	May 31, June 1	Experiment-1b Experiment 1a (pdf)	Fractional Distillation/Simple Distillation YouTube How to Build a Proper Still: part I How to Build a Proper Still: part II How to Run a Basic GC	I ^{1, 2}
	June 4, 5	Experiment 2 (docx) Experiment 2 (pdf)	Recrystallization YouTube How to pack a melting point capillary and how to measure a melting point How to Flute Filter Paper Images Apparatus 1 Apparatus 2	PR, C
	June 6, 8	Experiment 3 (docx) Experiment 3 (pdf)	Extraction of Caffeine from Tea YouTube Rotary Evaporation: part I Rotary Evaporation: part II Sublimation Some Instruction on how to do the arrow formalism soxhlet extraction	I ²
	June 11	Experiment 4 (DOC) (PDF) Experiment 18 (PDF)	Introduction to Spectroscopy YouTube D₂O Addition of Fumarate to Produce Malate Set-up Rxn IR-1 basics important for fall IR-2 IR-3 IR-4 IR-5 important for fall How to prepare sample for NMR How to Inject a Sample into the NMR at Bryn Mawr College How to Run NMR Sample at Bryn Mawr College part I How to Run NMR Sample at Bryn Mawr College part II How to solve a basic NMR Problem A practice NMR problem A practice NMR problem Solution to basic nmr problem no. 3 Solution to NMR Problem no. 4 Quiz	I, G
	June 12, 13	Experiment 4 (DOC) (PDF) Experiment 18 (PDF)	Introduction to Spectroscopy (Continued) D₂O Addition of Fumarate to Malate Run NMR YouTube Running NMR part 3 Run NMR	I,G
	June 14, 15	Experiment 6a Experiment 6b	Free Radical Substitution: Chlorination of chlorobutane YouTube Running a Simple GC at Bryn Mawr College How to Make a Micro-drying Apparatus	I
	June 18, 19	Electrophilic Addition PDF	Electrophilic Addition YouTube Making an Omlette – Microrecrystallization technique	F
	June 20,22	Experiment 7	Nucleophilic Substitution: Preparation of 1-Bromobutane	P,F
	June 25, 26		Oxidation of Isoborneol to Champhor	P,F

PR	Prelab only
C	Conference on results and postlab with instructor
P	Preparative experiment/write-up
I	Investigative experiment/write-up
F	Form write-up
G	Group experiment/write-up. Only one report per group.
1	There will be one report written for two parts of this experiment.
2	Limited write up. See specific instructions in lab book.

Under Construction