Chemistry 211, Schedule for Semester I, Fall 2011

Week	Dates	Experiment #	Experiment Title	Experiment Type
General Lab Information (docx) (pdf) Forces and Factors (docx) (pdf) Laboratory Equipment
1	9/04 - 9/06		No lab meeting this week.
2	9/10 - 9/13	Experiment 1a (docx) Experiment 1a (pdf)	General Lab Information Gas Chromatography/Steam Distillation Check-in YouTube Orientation/Safety Lecture-thermal burn and cut safety General safety: Chemical exposure: Fire safety: Thermal Cuts and Burns: How to Build a Proper Still: part I How to Build a Proper Still: part II How to Run a Basic GC Images Apparatus 1 Apparatus 2	I ^{1, 2}
3	9/17 - 9/20	Experiment-1b Experiment 1a (pdf)	Fractional Distillation/Simple Distillation YouTube How to Build a Proper Still: part I How to Build a Proper Still: part II How to Run a Basic GC	I ^{1, 2}
5	9/24 t- 9/27	Experiment 3 (docx) Experiment 3 (pdf)	Extraction of Caffeine from Tea YouTube Rotary Evaporation: part I Rotary Evaporation: part II Sublimation Some Instruction on how to do the arrow formalism soxhlet extraction	I ²
6	10/01 - 10/04	Experiment 5 (DOC) (PDF)	Separation and Identification of Unknown Mixture YouTube YouTube on separation of acids and bases	I, G
8	10/08 - 10/11	Experiment 4 (DOC) (PDF) Experiment 18 (PDF)	Introduction to Spectroscopy D₂O Addition of Fumarate to Produce Malate Set-up Rxn YouTube IR-1 basics important for fall IR-2 IR-3 IR-4 IR-5 important for fall How to prepare sample for NMR How to Inject a Sample into the NMR at Bryn Mawr College How to Run NMR Sample at Bryn Mawr College part I How to Run NMR Sample at Bryn Mawr College part II How to solve a basic NMR Problem A practice NMR problem A practice NMR problem Solution to basic nmr problem no. 3 Solution to NMR Problem no. 4 Spectroscpy as Imagery	I, G
7	10/15 - 10/18		Fall Break, rest, eat, have fun
9	10/22 - 10/25	Experiment 4 (DOC) (PDF) Experiment 18 (PDF) Experiment 10a (DOCX) Experiment 10a (PDF)	Introduction to Spectroscopy (Continued) D₂O Addition of Fumarate to Malate Run NMR Set up Diels Alder Reaction YouTube Running NMR part 3 Run NMR	I,G
10	10/29 - 11/01	Experiment 18 (PDF) Experiment 10a (DOCX) Experiment 10a (PDF)	Conference on D₂O Addition of Fumarate to Moderate Set-up Rxn Recrystallize Diels-Alder Product	F
11	11/13 -11/15(miss Monday)	Experiment 7	Nucleophilic Substitution: Preparation of 1-Bromobutane Quiz 1 (attachment) except Monday Section	P,F
12	11/19 - 11/22		Thanksgiving Week, Make-up Days
13	11/26, 11/27,11/28, 11/29, 11/30	Oxidation of Isoborneol to Camphor (PDF)	Oxidation of Isoborneol to Camphor	2
15	12/03 - 12/06	Experiment 6a Experiment 6b	Free Radical Substitution: Chlorination of chlorobutane YouTube Running a Simple GC at Bryn Mawr College How to Make a Micro-drying Apparatus Conference during Lab Quiz 2	I

PR	Prelab only
C	Conference on results and postlab with instructor
P	Preparative experiment/write-up
I	Investigative experiment/write-up
F	Form write-up
G	Group experiment/write-up. Only one report per group.
1	There will be one report written for two parts of this experiment.
2	Limited write up. See specific instructions in lab book.