Schedule of Experiments |
|||
date |
experiment title |
techniques |
|
| Sept. 3 | Introduction/Methylation of 5-Iodo-salicylic Acid | anaerobic synthesis, hazardous chemical use | |
| Sept. 10 | Amide Synthesis | anaerobic synthesis, hazardous chemical use | |
| Sept. 17 | Amide Purification | product purification by flash chromatography | |
| Sept. 24 | 2D NMR Analysis of Amide | advanced NMR techniques | |
| Oct. 1 | Synthesis of Molybdenum Carbonyls | anaerobic inorganic syntheses; FT-IR | |
| Oct. 8 | Structural Identity of Mo-Carbonyls by Vibrational Analysis | use of character tables in vibrational analysis | |
| Oct. 22 | Wilkinson’s Catalyst: synthesis & aldehyde reaction | organometallic synthesis, ESI-MS, FT-IR | |
| Oct. 29 | Wilkinson’s Catalyst: catalytic hydrogenation | organometallic catalyzed reaction, GC-MS | |
| Nov. 5 | Metal Catalyzed C-C Cross Coupling | catalytic reaction | |
| Nov. 12 | Models for Molybdenum Enzymes. 1 | FT-IR, 1H NMR, electronic spectroscopy | |
| Nov. 19 | Models for Molybdenum Enzymes. 2 | column chromatography | |
| DEC. 3 | Models for Molybdenum Enzymes. 3 | ESI-MS | |